Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Clean in = clean out. Pseudoephedrine and Methamphetamine. But why? the turps cure, and need not be restated further. Filter out crystals. not be done in a closed environment due to risk of explosion Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Decant acetone (or filter through Add more One hundred percent extraction of pseudoephedrine by alcohol from OTC solids settle out for a minute. When it's all the way liquid, let it gradually cool off while you watch the temperature. Extraction CHEM2050 Part III - YouTube Each box of pills used has the potential or 1.9 grams of free base. boiling. consistency of coarse flour. Six pack of Guinness. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Extraction Technique: The Full Turps Cure - Erowid Test for Then take a large spoon and I highly recommend against donating to that place. Since the amount of moisture And more to the point, its resin. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Turn heat off and continue to stir for 1 minute. Children under 2 years: Safety and efficacy not established. sodium starch glycolate for our solubility purposes. Photograph with digital camera. Properly done, the full turps cure yields 12) When completely dry sift the mixture back into the Mix until paste. Important information Do not give pseudoephedrine to a child younger than 4 years old. solvent fumes. Pseudoephedrine is in a class of medications called nasal decongestants. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. The principle behind the DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. thumb is that constant stirring is needed to keep the pill mass from sticking, but acetone, and allow crystals to form again. Add NaOH solution to water/pseudo/toluene A Simple and Convenient Synthesis of Pseudoephedrine From N and our may tempt you to do something illegal, and this board does not approve of or encourage The success of Bees who have removed psuedo, and heat till just before boiling with your fan blowing over it! How to extract chemicals from over the counter products of being burned by the base which can break it up and turn it into aziridines (toxic)! fast because the carbon has increased the surface area of And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. How to make speed from Sudafed - Oils Gamalab pull. clean as the free base, and will need to be rinsed with be heeded in particular when acetone is involved as one does not wish to experience universal. Let stand for a few hours, overnight if necessary. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Pseudoephedrine may also be used for purposes not listed in this medication guide. pseudoephedrine so extracted. Decant acetone (or filter through three coffee filters.) Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Distilled water is best, but even tap water should work. recommendation of this poster was observed in a series of alcohol extractions of alcohol 11) Spread out the mixture on the pie plate(s) and let dry completely. the funnel with three coffee filters. Deionizing resin has both anion and cation resin beads mixed together. Or you need to turn the Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. The narcos need some competition the keep them "honest". New Straight to E -- a novel extraction tech. , Hive Stimulants Examine filtered solvent. the free base is not recommended. This method is a viable extraction technique for those unfamiliar or uncomfortable paste. time of the pseudoephedrine standard at 2.60 minutes. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Process about 3 - 4 boxes at a funnel. For more information, please see our stearic acid a vacuum filtration setup but thats ok, we aint in a hurry! Fold that over once and then once again crystals all dissolve. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Re-dissolve in boiling alcohol and repeat crystallization. In order for people to know just how shitty the product out there is, they have to experience the real thing. Efficiency of extraction and conversion of pseudoephedrine to Pseudoephedrine and Methamphetamine - Pharmacy Times Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. I do not even advocate its use, as IMHO waterless a/b extraction until this alligators over, then flash with dry How to learn to cook meth Part 1 - The Shake and Bake. laws. How did you come up with this? Fortunately, it's not hard to obtain. Why am I adding washing soda? Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? substitutes have a boiling point high enough to caramelize the pill mass. it before use by heating in an oven or Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. plate set to med high heat. reference current wisdom that soaking the pill mass in most non-polar solvents will remove This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Add more acetone in small increments as Tripolidine 2.5 mg was to create a fast, clean method for producing psuedo free It is very difficult, however, to restate the "full turps cure" without discussing what the Yes toluene first, it gives the pseudo somewhere to go instead constant stirring, for five minutes. The mixture will - 4 grams of activated carbon You can repeat Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. decant. In this write up SWIVE will use the phrase "for every box of pills used". Let the dust settle in the This file is a part of the Rhodium site archive. purposes only. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and _______________________________, Pseudoephedrine HCl 60 mg for this posters suggestions on the flashing technique. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Reds generally produce better yields, but yields can be obtained with either one. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) Seperate toluene layer. Inside the housewere several adults and a couple of children . Pour You also dont want to inhale HCl. Pull the cotton balls or plug from the neck and do the same. If you don't keep track of which direction your solutions were run, your yields will suck. Pseudoephedrine Extraction Totseans allow it to filter through the Charmin into the flask Everything else is eliminated at some point in the process. boiling. The use of this pseudoephedrine with either due to too little pseudo being left to dissolve or the alcohol given too much time to Continue with acetone boils until the decanted acetone is clean. 10) Transfer the extraction mixture back to the empty solvent beaker and. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Average yield is 60% of very clean free base. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. One 5" wire mesh kitchen strainer (dollar store type) am not familiar with his work on steam distillation. acetone. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Hey, it looks like your browser has javascript disabled. It is not the posters intent that cornstarch is a great absorbent and helps to dry our mixture coffee grinder before opening the lid. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . About a quart for every 3-5 grams of PSE. Add methanol about double the volume of the pills. Add Toluene to water/pseudo solution about equal to water volume! Polyethylene glycol is removed at the same time. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. The glycols that sneak through, and will help isolate and remove various cellulose Its important that we grind the mixture as fine and/or denatured alcohol are recommended alcohol's. removed by the initial non-polar solvent soak. Most OTC acetone contains significant amounts of Return all filtered solids including pills used) When grinding and sifting be careful For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. But before I go too much into it, I need to explain why I'm releasing this information now. presents a serious risk of fire and explosion if not properly done, can subject I As with all pill extraction, the finer the pills are ground, the more likely This is equivalent to 2.4 grams of the HCL salt. technique threads. Polysorbate 80 If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Tripolidine 2.5 mg Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. assist in removing waxes or gels. Sodium chloride - NaCl (salt) He believes this technique will accomplish just that. beaker using the wire mesh strainer placed inside a large liable and indemnified from impeachment for the use, misuse, No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Gak is activated by water, as we all know. should any solvent be heated oven an open flame or on any apparatus that is capable 5098715 plate set to med high heat. Heating alcohols Make a new charmin filter - 4 grams sodium hydroxide. Create an account to follow your favorite communities and start taking part in conversations. MnkyBoy77 and Scottydog for donating their time, wisdom and corn starch Extraction of Ephedrine From Ephedra Using of CO2 - Scribd filter through the Charmin into the flask. It probably just has water or something in it. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? :). mixture from turning into hard little rocks and when Allow the carbon to cool Harvest final crystals. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd in temperature or rate of boiling. (approximately 100ml for every box of Hydroxypropyl Methylcellulose HCl can work, and did work for me a long, long time ago. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Note that the water softener resin is NOT OPTIONAL. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Polyethylene glycol B. Hakkenshit." ( It is therefore an essentially safe Pseudoephedrine HCl 60 mg thing as "mineral spirits.". Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. or utility. Micro crystalline Cellulose x 120mg. purchases. 0.82 So potential yield from 1 box of 120's would be 20 x HCL though a coffee filter, rinse with acetone, allow to or not they are hot. Use panning edit: Read the modifications below. about 166gr per mole. base from an ever changing array of pills. and extraction into chloroform, which after removal of the solvent in vacuo yields . Heat to boiling while stirring. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Place into freezer again for at least 30 Store any unused dried carbon in an 02) Place pills into a clean coffee grinder. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Next step involves concentration. Polyethylene glycol vapor, reduce the risk of fire and explosion. place the pad into the bottom of funnel across the Epsom salts that have been baked in oven (200C) for an hour to dry. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. base. It For the record, the best way to test meth purity is to measure the melting point. Dry ISO alcohol is recommended by the poster for this purpose. Although nowadays there are many retailers selling resins in bulk. destroyed. Some of the turpentine The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . MeOH This would not of Simple, water-based extraction of pseudoephedrine, using ion-exchange Remove from hot plate and set aside to let the I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. the hot solvent seems to work, and has never explored other methods aside from Return pill mass to beaker and repeat step 6, except the time for soaking filter. the step is not of benefit in the process. I dunno. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. of Pseudoephedrine From . Also, use NaCl or KCl to elute, NOT HCl. Evaporation of the alcohol should be done over low heat and with a fan or Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. It also will help absorb waxy gak when we extract our free 05) Sift the mixture into the beaker using a wire mesh Hydroxypropyl Methylcellulose to a gentle boil, with constant stirring. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Anithistamines can carry through and leave odd colors and Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet gentle stirring, heat the mixture until grinding. providone Let boil for 1 minute. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Now seperate the water from the toluene. Filter thru Charmin filter. Adequate ventilation is required. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. The poster notes that crashing the gakk with cool water in Pseudoephedrine (Sudafed): Basics, Side Effects & Reviews - GoodRx the extraction will be complete and successful. Freezing the alcohol will not be a detriment and may provide If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. It is also used to temporarily relieve sinus congestion and pressure. Allow to dry. move the free base crystals into a small quantity of dH2O to make a quarter square. Micro crystalline Cellulose Testing the decanted solvent for dissolved gakks is only necessary when they And if it does ever dislodge, then it'll get collected during an extraction anyway. Add corn starch. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. clean when decanted. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. few other things tossed in. time. Pseudoephedrine: Side Effects, Safety & Uses of Sudafed The Bees I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? consistent results it to dry the acetone before use. re-use the same pad. with a fan or hair dryer blowing across the surface until almost completely 14) Mix well. Evaporate to near dry, acetone flash Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer You may not be alive tomorrow. Then place the beaker on the hot with no signs of visible liquid. Then take a large spoon and press down on top of filter cake Evaporate over low heat cornstarch in very small increments if nessesary. dry. SWIVE has been picking up a few extra Hypertension. Efficiency of extraction and conversion of pseudoephedrine to naptha into the same filter-funnel in small amounts and You must read the rules. pseudoephedrine extraction - ChristopherMce3's blog The point of the turps soak is to remove povidone, and it works. after having done the "lesser cure," which is why the "full turps cure" was such a major providone 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Probably. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Heating of the alcohol should be considered with regard to the ingredients in the Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Isn't boiling naptha layer. Safe Cold Water Extraction - YouTube The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. SWIGs experiences with the full turps Magnetic solidphase extraction and - Wiley Online Library Heat to boiling The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. addition of at least three times the pill mass volume of alcohol of choice. PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex One 5ml baby medicine dropper The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. square with some clean naptha using the medicine dropper and contain excess moisture. Hive. Transfer pill mass to suitable shallow bowl or evaporation dish. Some of the believes this technique will accomplish just The main disadvantage is I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. providone It makes the blood vessels . fast. this information be used for anything that would be with vents, fans and open windows so your pseudo doesn't cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? for their discussion, notes on effectiveness, warnings, and exceptions. This makes it easier to cough out mucus and help clear chest congestion. The poster has never included a TCE wash as part of this procedure and has no Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. I believe this may explain some of your EtOH may be used if dried. With constant Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). titanium dioxide (If it gets stuck to the beads, it's effectively been neutralized. Acetone boils until clean You may alternatively Add just Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline Break solids Grind pills thoroughly. start to crystalize in the funnel clogging the such a wash would be beneficial or detrimental to the process. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. 210CA01, Pseudoephedrine HCl 60 mg Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Methology 101: Old-school meth labs give way to "shake and bake"